Journal of Fluorine Chemistry p. 233 - 248 (1991)
Update date:2022-09-26
Topics:
Paciorek, K. J. L.
Masuda, S. R.
Shih, J. G.
Nakahara, J. H.
Mono- and di-iodoperfluoroalkylethers were synthesized and their reactions, as well as those of iodofluoroalkanes, with 4-iodobenzil were investigated.The formation of C8F17C6H4CHO, C8F17C6H4CO2H, C8F17C6H4COCOC6H5, and C8F17OCF2CF2C6H4COCOC6H5 proceeded readily.No C8F17OCF2C6H4COCOC6H5 was produced from the reaction of C8F17OCF2I with 4-iodobenzil in the presence of copper bronze.Low yields of bridged bisbenzils were obtained from the coupling rections of ICF2CF2O(CF2)5OCF2CF2I and I(CF2CF2O)5CF2CF2I with 4-iodobenzil.Based on by-products formed, the operative mechanisms are postulated.
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(1991)
