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THE SYNTHESIS OF PERFLUOROALKYL AND PERFLUOROALKYLETHER SUBSTITUTED BENZILS

DOI: 10.1016/S0022-1139(00)82343-X

Source and publish data:

Journal of Fluorine Chemistry p. 233 - 248 (1991)

Update date:2022-09-26

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Authors:

Paciorek, K. J. L.Paciorek, K. J. L.

Masuda, S. R.Masuda, S. R.

Shih, J. G.Shih, J. G.

Nakahara, J. H.Nakahara, J. H.

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Article abstract of DOI:10.1016/S0022-1139(00)82343-X

Mono- and di-iodoperfluoroalkylethers were synthesized and their reactions, as well as those of iodofluoroalkanes, with 4-iodobenzil were investigated.The formation of C8F17C6H4CHO, C8F17C6H4CO2H, C8F17C6H4COCOC6H5, and C8F17OCF2CF2C6H4COCOC6H5 proceeded readily.No C8F17OCF2C6H4COCOC6H5 was produced from the reaction of C8F17OCF2I with 4-iodobenzil in the presence of copper bronze.Low yields of bridged bisbenzils were obtained from the coupling rections of ICF2CF2O(CF2)5OCF2CF2I and I(CF2CF2O)5CF2CF2I with 4-iodobenzil.Based on by-products formed, the operative mechanisms are postulated.

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Full text of DOI:10.1016/S0022-1139(00)82343-X

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Product name:1-{4-[2-(1,1,2,2,3,3,4,4,5,5-Decafluoro-5-{1,1,2,2-tetrafluoro-2-[4-(2-oxo-2-phenyl-acetyl)-phenyl]-ethoxy}-pentyloxy)-1,1,2,2-tetrafluoro-ethyl]-phenyl}-2-phenyl-ethane-1,2-dione

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