Synthesis p. 635 - 636 (1989)
Update date:2022-08-06
Topics:
Albeck, M.
Tamari, T.
Sredni, B.
Ammonium trichloro(dioxyethylene-O,O')tellurate(IV) (AS-101) was synthesized by refluxing tellurium(IV) chloride and ethylene glycol in acetonitrile, or by refluxing tellurium(IV) chloride and ammonium chloride in ethylene glycol.A mechanism for the reaction is suggested.X-ray data for AS-101 are given.Replacing ammonium chloride by potassium chloride yielded the potassium salt; however, with sodium chloride the sodium salt was not obtained.
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