First synthesis of a strained 14-membered biaryl ether lactone by macrolactonization

DOI: 10.1016/S0040-4039(00)93554-8

Source and publish data:

Tetrahedron Letters p. 5781 - 5784 (1991)

Update date:2022-08-03

Topics:

Authors:

Justus Justus

Steglich

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Article abstract of DOI:10.1016/S0040-4039(00)93554-8

The synthesis of biaryl ether lactone 3 by macrolactonization of hydroxy acid 8 under defined Mitsunobu conditions is described. In accord with the literature, attempts to cyclize 8 via carboxyl activation failed.

Full text of DOI:10.1016/S0040-4039(00)93554-8

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