Synthesis of (-)-δ-N-Normethylskytanthine

DOI: 10.1016/0040-4039(91)80484-N

Source and publish data:

Tetrahedron Letters p. 7233 - 7236 (1991)

Update date:2022-07-30

Topics: Synthesis Catalyst Solvent Chromatography Reactants Spectroscopy Extraction

Authors:

Cid, M. M.

Eggnauer, U.

Weber, H. P.

Pombo-Villar, E.

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Article abstract of DOI:10.1016/0040-4039(91)80484-N

(-)-δ-N-Normethylskytanthine (1) has been synthsised from (1R,4R,1'S)-2-(phenylethyl)-2-azabicyclo<2.2.1>hept-5-ene (2) which undergoes a ketene-amino-Claisen rearrangement by reaction with dichloroketene to generate (1S,6R,1'S)-3-(phenylethyl)-5,5-dichlo

Full text of DOI:10.1016/0040-4039(91)80484-N

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Product name:(-)-(1S,6R,1'S)-5,5-dichloro-3-(1'-phenylethyl)-3-azabicyclo<4.3.0>non-7-en-4-one

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