Tetrahedron p. 1417 - 1426 (1992)
Update date:2022-08-02
Topics:
Dombroski
Snider
Oxidative free-radical cyclizations of γ,γ-(bis)allylic acetoacetates demonstrate that 1,1-disubstituted double bonds are much more reactive than mono- or chloroalkyl-substituted double bonds. The products isolated suggests that bicyclo[3.2.1]octanes 25, 31, 33 and 36 are formed from boat cyclohexyl radical 42 and tandem cyclization products 30, 37 and 38 are obtained from boat cyclohexyl radical 41.
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Doi:10.1002/hlca.19910740420
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(2017)