Synthese und Charakterisierung von 1,3-disubstituierten Decamethylcyclohexasilanen

DOI: 10.1016/0022-328X(92)83096-Z

Source and publish data:

Journal of Organometallic Chemistry p. 335 - 343 (1992)

Update date:2022-08-05

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Authors:

Hengge, E.

Eibl, M.

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Article abstract of DOI:10.1016/0022-328X(92)83096-Z

The reaction of SbCl5 with Si6Me12 yields 1,3- and 1,4-Cl2Si6Me10.In order to isolate these isomers, a mixture of 1,3- and 1,4-2Si6Me10 was synthesized and separated by fractional extraction with benzene.The structure of 1,3-2Si6Me10 has been revealed by 29Si-INEPT-INADEQUATE spectroscopy.Starting from 1,3-2Si6Me10, the compounds 1,3-Cl2Si6Me10, 1,3-Br2Si6Me10 and 1,3-H2Si6Me10 were synthesized and characterized.

Full text of DOI:10.1016/0022-328X(92)83096-Z

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