A stereospecific approach towards the synthesis of 2-deoxy α- and β-glycosides based on a 1,2-ethyl (phenyl) thio group migration

DOI: 10.1016/S0040-4020(01)80165-4

Source and publish data:

Tetrahedron p. 6501 - 6514 (1993)

Update date:2022-07-29

Topics:

Authors:

Zuurmond

Van Der Klein

Van Der Marel

Van Boom

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Article abstract of DOI:10.1016/S0040-4020(01)80165-4

Iodonium ion (NIS/TfOH)-assisted glycosylation of a sugar acceptor with properly protected ethyl (phenyl) 2-O-phenoxythiocarbonyl 1-thio-β-D-gluco- or 1-thio-α-D-mannopyranoside donors gives the respective 1,2-trans linked 2'-ethyl (phenyl) thio-2'-deoxy-α-D-manno- or β-D-glucopyranosides.

Full text of DOI:10.1016/S0040-4020(01)80165-4

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