Tetrahedron Letters p. 4831 - 4834 (1993)
Update date:2022-09-26
Topics:
Lee, Eun
Tae, Jin Sung
Lee, Chulbom
Park, Cheol Min
β-Alkoxyacrylates were found to be exceptionally efficient radical acceptors in radical-mediated intramolecular cyclizations. For example, reaction of 5-bromo-2-pentanol with ethyl propiolate, tributylstannane-mediated radical cyclization, and hydrolysis yielded (±) (cis-6-methyltetrahydropyran-2-yl)acetic acid, a known component of civet.
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Doi:10.1021/jo00079a033
(1993)Doi:10.1016/S0040-4039(00)79301-4
(1993)Doi:10.1016/j.bmcl.2013.11.054
(2014)Doi:10.1016/j.tetlet.2018.12.018
(2019)Doi:10.1016/j.tet.2009.09.060
(2009)Doi:10.1002/jhet.5570300226
(1993)
