Synlett p. 1271 - 1272 (1997)
Update date:2022-09-26
Topics:
Enders, Dieter
Klein, Daniela
Raabe, Gerhard
Runsink, Jan
The diastereo- and enantioselective syntheses of various α′-t-butyldimethylsilyl-α-iodo ketones 4a-h is described. The carbon iodine bond formation is achieved using trifluoroiodomethane as the electrophilic iodination reagent. The iodo ketones 4 are obtained in good yields and with excellent diastereo- and enantiomeric excesses (de,ee ≥ 98%).
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