Carbohydrate Research p. 61 - 80 (1994)
Update date:2022-09-26
Topics:
Fernandez, Paloma
Jimenez-Barbero, Jesus
Martin-Lomas, Manuel
The synthesis of all possible monomethyl ethers of methyl β-lactoside (1) has been performed from 1 in a straightforward way, making use of the different reactivity of the hydroxyl groups in alkylation and stannylation reactions.In addition, the deoxyfluoro derivatives of 1 at positions, 6, 3',4',epi-4', and 6' have been prepared by reaction of the appropriate substrates with diethylaminosulfur trifluoride or tetrabutylammonium fluoride.Finally, the 6-deoxyiodo and 6'-bromodeoxy analogues of 1 have also been prepared.
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(1994)Doi:10.1021/jo500032k
(2014)Doi:10.1080/00397919408011722
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