Chemistry Letters p. 539 - 542 (1994)
Update date:2022-07-29
Topics:
Tsunoda, Tetsuto
Otsuka, Junko
Yamamiya, Yoshiko
Ito, Sho
N,N,N',N'-Tetramethylazodicarboxamide, (TMAD), was found to be more versatile in the Mitsunobu reaction than traditional diethyl azodicarboxylate or recently developed 1,1'-(azodicarbonyl)dipiperidine, when used in combination with tributylphosphine in benzene.The usefulness of the reagent was demonstrated by the highly efficient two-step synthesis of benzylcrotylamine from N-benzyltrifluoroacetamide.
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(1994)Doi:10.1021/ol4037133
(2014)Doi:10.1021/jo4025732
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