
Journal of Organic Chemistry p. 2927 - 2929 (1994)
Update date:2022-08-05
Topics:
An, Yi-Zhong
Rubin, Yves
Schaller, Christophe
McElvany, Stephen W.
Diethynylmethanobuckminsterfullerene (1a and 13C-labeled 1b) has been prepared by reaction of the lithium salt of 1,5-bis(trimethylsilyl)-1,4-pentadiyn-3-one (p-toluenesulfonyl)hydrazone (5a/b) with C60 followed by desilylation and characterized by NMR, IR, UV-vis, and CI-TQMS spectroscopies.
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