Synthesis of Protected 4-Oxopipecolic Acid and 4-Oxolysine using a Palladium-catalysed Coupling Process

DOI: 10.1016/S0040-4039(00)73372-7

Source and publish data:

Tetrahedron Letters p. 4417 - 4418 (1994)

Update date:2022-07-30

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Authors:

Jackson, Richard F. W.

Graham, Lisa J.

Rettie, Alan B.

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Article abstract of DOI:10.1016/S0040-4039(00)73372-7

Reaction of the L-serine derived zinc reagent 3 with acryloyl chloride gave 4-oxo amino acid 4, with no evidence of products arising from conjugate addition.Treatment of the adduct 4 with benzylamine gave protected 4-oxolysine 5 directly.Reduction of the

Full text of DOI:10.1016/S0040-4039(00)73372-7

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