Chemical and Pharmaceutical Bulletin p. 1437 - 1441 (1994)
Update date:2022-08-05
Topics:
Kurita
Ishii
Yasuike
Tsuchiya
The Group 14 (Si, Ge, and Sn), Group 15 (P, As, Sb, and Bi), and Group 16 (Se and Te) 2-trimethylsilyl-1-benzometalloles (7) were prepared by the reaction of the corresponding metal reagents with β,o-dilithio-β-trimethyl- silylstyrene intermediate (6), which was derived from phenylacetylene or o- bromoiodobenzene via three steps. The trimethylsilyl group in 7 could be readily removed by treatment with tetrabutylammonium fluoride to give the C- unsubstituted 1-benzometalloles (10).
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