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61-54-1

Basic Information
CAS No.: 61-54-1
Name: 1H-Indole-3-ethanamine
Molecular Structure:
Molecular Structure of 61-54-1 (1H-Indole-3-ethanamine)
Formula: C10H12N2
Molecular Weight: 160.24
Synonyms: Indole,3-(2-aminoethyl)- (8CI);2-(1H-Indol-3-yl)ethanamine;2-(3-Indolyl)ethylamine;3-(2-Aminoethyl)-1H-indole;3-(2-Aminoethyl)indole;b-(3-Indolyl)ethylamine;
EINECS: 200-510-5
Density: 1.158 g/cm3
Melting Point: 113-116 °C(lit.)
Boiling Point: 378.766 °C at 760 mmHg
Flash Point: 187.672 °C
Solubility: negligible
Appearance: White to orange crystalline powder
Hazard Symbols: IrritantXi
Risk Codes: 20/21/22-36/37/38-41
Safety: 24/25-36/37/39-26
Transport Information:
PSA: 41.81000
LogP: 2.36940
Synthetic route
31731-23-4

3-(2-nitroethyl)indole

61-54-1

tryptamine

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In methanol under 760.051 Torr; for 24h;98%
With sodium hypophosphite monohydrate; 5%-palladium/activated carbon; hypophosphorous acid In 2-methyltetrahydrofuran; water for 7h; Sonication; chemoselective reaction;94%
With palladium 10% on activated carbon; hydrogen In ethanol at 20℃; for 15h;86.94%
73-22-3

L-Tryptophan

61-54-1

tryptamine

Conditions
ConditionsYield
With pyridoxal 5'-phosphate; aromatic L-amino acid decarboxylase In various solvent(s) at 30℃; for 48h;98%
cyclohexenone In various solvent(s) at 154℃; for 1.5h;92.3%
With L-amino acid decarboxylase from Micrococcus percitreus AJ 1065; NH4OH-NH4Cl buffer; pyridoxal 5'-phosphate In water at 30℃; for 0.5h; Product distribution; study of the inhibition of the enzyme by various amino acids and amines, inhibition of L-dopa in different buffer solutions;
1042701-07-4

tert-butyl 4-(2-aminophenyl)-2,3-dihydro-1H-pyrrole-1-carboxylate

61-54-1

tryptamine

Conditions
ConditionsYield
Stage #1: tert-butyl 4-(2-aminophenyl)-2,3-dihydro-1H-pyrrole-1-carboxylate With trifluoroacetic acid In dichloromethane at 0 - 25℃; Inert atmosphere;
Stage #2: With sodium hydrogencarbonate In water pH=> 7; Inert atmosphere; Saturated solution;
98%
With trifluoroacetic acid In dichloromethane at 0 - 25℃; for 2h; Inert atmosphere;98%
86658-78-8

N-tosyl tryptamine

61-54-1

tryptamine

Conditions
ConditionsYield
With pyrrolidine; samarium diiodide; water In tetrahydrofuran at 20℃; Inert atmosphere;94%
38750-13-9

(2-indol-3-yl-ethyl)-carbamic acid benzyl ester

61-54-1

tryptamine

Conditions
ConditionsYield
With hydrogen; palladium In ethanol; ethyl acetate under 22502.3 Torr;94%
120-72-9

indole

56-45-1

L-serin

61-54-1

tryptamine

Conditions
ConditionsYield
Stage #1: indole; L-serin With engineered tryptophan synthase In methanol; aq. phosphate buffer at 75℃; for 12h; pH=8.0; Enzymatic reaction;
Stage #2: With pyridoxal 5'-phosphate; Ruminococcus gnavus L-tryptophan decarboxylase In methanol; aq. phosphate buffer at 37℃; pH=8.0; Enzymatic reaction;
92%
3156-51-2, 51870-94-1

3-[(E)-2-nitroeth-1-enyl]-1H-indole

61-54-1

tryptamine

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran for 7h; Reflux;89%
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 6h; Inert atmosphere;83.5%
With lithium aluminium tetrahydride; diethyl ether
103549-24-2

tert-butyl [2-(1H-indol-3-yl)ethyl]carbamate

61-54-1

tryptamine

Conditions
ConditionsYield
In various solvent(s) at 150℃; for 1h; microwave irradiation;88%
With 1,1,1,3',3',3'-hexafluoro-propanol at 150℃; for 1h; Microwave irradiation;88%
With 1,1,1,3',3',3'-hexafluoro-propanol at 150℃; for 1h; Microwave irradiation;88%
4753-09-7

N-benzoyltryptamine

61-54-1

tryptamine

Conditions
ConditionsYield
With sodium hydroxide In water; ethylene glycol82%
879-37-8

3-indolylacetamide

61-54-1

tryptamine

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran Reflux;81%
With lithium aluminium tetrahydride
With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; for 3h; Inert atmosphere;
1016-47-3

N-Acetyltryptamine

61-54-1

tryptamine

Conditions
ConditionsYield
With ammonium bromide; ethylenediamine at 80℃; for 5h; Microwave irradiation; Inert atmosphere; neat (no solvent);81%
With recombinant Arabidopsis thaliana histone deacetylase 14 In aq. buffer at 30℃; pH=8; Reagent/catalyst; Enzymatic reaction;
126402-58-2

4-(4,8-Dimethoxy-naphthalen-1-ylmethyl)-N-[2-(1H-indol-3-yl)-ethyl]-benzenesulfonamide

61-54-1

tryptamine

Conditions
ConditionsYield
With ammonia borane In ethanol Irradiation;78%
771-51-7

indole-3-acetonitrile

61-54-1

tryptamine

Conditions
ConditionsYield
With lithium aluminium tetrahydride In diethyl ether at 0℃; for 12h; Inert atmosphere;75%
With samarium diiodide; water; triethylamine In tetrahydrofuran at 20℃; for 0.0833333h; Inert atmosphere;74%
With lithium aluminium tetrahydride; diethyl ether
63778-37-0

3-(2-azidoethyl)-1H-indole

61-54-1

tryptamine

Conditions
ConditionsYield
Stage #1: 3-(2-azidoethyl)-1H-indole With formic acid; tris(2,2'-bipyridyl)ruthenium dichloride; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; N-ethyl-N,N-diisopropylamine In methanol; N,N-dimethyl-formamide at 25℃; for 24h; Irradiation;
Stage #2: With di-tert-butyl dicarbonate; triethylamine In methanol; N,N-dimethyl-formamide at 25℃; for 12h;
72%

3-((Z)-2-Nitro-vinyl)-1H-indole

61-54-1

tryptamine

Conditions
ConditionsYield
With hydrogenchloride; iron In methanol; water for 0.5h; Heating;71%
61-54-1

tryptamine

Conditions
ConditionsYield
In diphenylether for 10h; Heating;63%
With Catharanthus roseus tryptophan decarboxylase In aq. phosphate buffer at 25℃; pH=7.5; Kinetics; Reagent/catalyst; Enzymatic reaction;
60716-71-4

2-(2,3-dihydro-2-oxo-3-indolyl)ethylamine

61-54-1

tryptamine

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 2h; Inert atmosphere;62%
54322-20-2

4-chloro-1-hydroxy-1-butanesulfonate sodium

59-88-1

phenylhydrazine hydrochloride

61-54-1

tryptamine

Conditions
ConditionsYield
With disodium hydrogenphosphate In ethanol at 70℃; for 6h;61%
With disodium hydrogenphosphate In ethanol at 70℃; for 6h;
74321-36-1

(3-Indolyl)acetaldehyd-dimethylhydrazon

61-54-1

tryptamine

Conditions
ConditionsYield
With hydrogen; rhenium; nickel In methanol under 760 Torr; for 12h; Ambient temperature;52%
771-51-7

indole-3-acetonitrile

A

61-54-1

tryptamine

B

168209-33-4

1-(3-methyl-1H-indole)-1,2,3,4-tetrahydro-β-carboline

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In methanol for 96h;A 38%
B 31%
771-51-7

indole-3-acetonitrile

A

61-54-1

tryptamine

B

13078-91-6

3-(2-aminoethyl)-2,3-dihydro-1H-indole

Conditions
ConditionsYield
With ammonia; nickel at 100℃; under 66195.7 Torr; Hydrogenation;
3389-21-7

3-(2-bromoethyl)-1H-indole

61-54-1

tryptamine

Conditions
ConditionsYield
With ammonia; water
6346-09-4

4-aminobutyrylaldehyde diethylacetal

100-63-0

phenylhydrazine

61-54-1

tryptamine

Conditions
ConditionsYield
With zinc(II) chloride
5548-10-7

indole-3-glyoxylamide

61-54-1

tryptamine

Conditions
ConditionsYield
With lithium aluminium tetrahydride
With lithium aluminium tetrahydride In tetrahydrofuran Heating;
With lithium aluminium tetrahydride In 1,4-dioxane for 34h; Heating;0.90 g
With lithium aluminium tetrahydride In 1,4-dioxane for 50h; Heating;

N-Methylhomoisoleucyltryptamine

A

61-54-1

tryptamine

(-)-N-Methylhomoisoleucine

Conditions
ConditionsYield
With hydrogenchloride for 24h; Heating;
96014-22-1

(E)-N-(2-(1H-indol-3-yl)ethyl)-3-(4-hydroxy-3-methoxyphenyl)acrylamide

A

61-54-1

tryptamine

B

1135-24-6

(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid

Conditions
ConditionsYield
In sodium hydroxide
808134-47-6

2-[1-(phenylsulfonyl)-1H-indol-3-yl]ethanamines

61-54-1

tryptamine

Conditions
ConditionsYield
With sodium hydroxide for 2h; Heating; Yield given;
212707-60-3

(E)-N-(2-(1H-indol-3-yl)ethyl)-3-(4-hydroxyphenyl)acrylamide

A

61-54-1

tryptamine

B

7400-08-0

p-Coumaric Acid

Conditions
ConditionsYield
In sodium hydroxide
61-54-1

tryptamine

103-71-9

phenyl isocyanate

32585-51-6

N-[2-(1H-indol-3-yl)ethyl]-N'-phenylurea

Conditions
ConditionsYield
Stage #1: tryptamine; phenyl isocyanate In dichloromethane at 60℃;
Stage #2: With isatoic anhydride-N-(CH2)3-C8F17 In dichloromethane at 60℃; for 2.5h;
100%
In dichloromethane at 60℃; for 5h; Inert atmosphere; Sealed reaction vessel;98%
61-54-1

tryptamine

501-53-1

benzyl chloroformate

38750-13-9

(2-indol-3-yl-ethyl)-carbamic acid benzyl ester

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In chloroform at 20℃; for 1h;100%
With N-ethyl-N,N-diisopropylamine In chloroform at 0 - 20℃; for 1h;100%
With sodium hydroxide In tetrahydrofuran97%
61-54-1

tryptamine

79-04-9

chloroacetyl chloride

52191-26-1

2-chloro-N-<2-(indol-3-yl)ethyl>acetamide

Conditions
ConditionsYield
With potassium carbonate In dichloromethane Ambient temperature;100%
In dichloromethane100%
With triethylamine In tetrahydrofuran at 20℃; for 6h; Cooling with ice; Inert atmosphere;96%
61-54-1

tryptamine

98-59-9

p-toluenesulfonyl chloride

86658-78-8

N-tosyl tryptamine

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 2h;100%
With triethylamine In dichloromethane at 0 - 20℃;99%
With triethylamine In dichloromethane at 0 - 20℃; for 2h;99%
61-54-1

tryptamine

1821-12-1

4-Phenylbutyric acid

102181-30-6

N-(2-(1H-indol-3-yl)ethyl)-4-phenylbutanamide

Conditions
ConditionsYield
With Trimethyl borate In acetonitrile at 80℃; for 15h;100%
With tris(2,2,2-trifluoroethyl) borate In acetonitrile at 80℃; for 15h;70%
at 180℃;
61-54-1

tryptamine

109-94-4

formic acid ethyl ester

6502-82-5

Nb-formyltryptamine

Conditions
ConditionsYield
for 24h; Reflux;100%
for 6h; Reflux;100%
With triethylamine In methanol at 100℃; for 16h; Inert atmosphere;97%
61-54-1

tryptamine

541-41-3

chloroformic acid ethyl ester

67909-99-3

ethyl 2-(1H-indole-3-yl)ethylcarbamate

Conditions
ConditionsYield
With triethylamine In 1,4-dioxane Ambient temperature;100%
With triethylamine In dichloromethane at 0℃; Inert atmosphere;99.4%
With sodium hydroxide In chloroform for 3h;95%
61-54-1

tryptamine

100-52-7

benzaldehyde

16979-93-4

N-benzylidene-2-(1H-indol-3-yl)ethylamine

Conditions
ConditionsYield
In toluene at 20℃; for 12h;100%
In methanol at 25℃; for 16h;70%
With molecular sives 4A In dichloromethane Ambient temperature;
61-54-1

tryptamine

922-67-8

propynoic acid methyl ester

194150-88-4

(E)-3-[2-(1H-Indol-3-yl)-ethylamino]-acrylic acid methyl ester

Conditions
ConditionsYield
In tetrahydrofuran for 5h; Ambient temperature;100%
61-54-1

tryptamine

140-88-5

ethyl acrylate

14487-98-0

3-<<2-(1H-indol-3-yl)ethyl>amino>propanoic acid ethyl ester

Conditions
ConditionsYield
In ethanol for 1h; Reflux;100%
In ethanol at 0℃; for 24h;83%
In tetrahydrofuran at 20℃; for 12h;83%
In ethanol at 0 - 20℃;80%
In ethanol
61-54-1

tryptamine

79-22-1

methyl chloroformate

58635-45-3

methyl 2-(1-H-indol-3-yl)ethylcarbamate

Conditions
ConditionsYield
With sodium hydroxide In dichloromethane; water at 0℃;100%
With triethylamine100%
With sodium hydroxide In ethyl acetate at 25℃; for 0.5h;95%
61-54-1

tryptamine

24424-99-5

di-tert-butyl dicarbonate

103549-24-2

tert-butyl [2-(1H-indol-3-yl)ethyl]carbamate

Conditions
ConditionsYield
With triethylamine In 1,4-dioxane for 1h;100%
With guanidine hydrochloride In ethanol at 35 - 40℃; for 0.05h;100%
With amberlyst-15 In ethanol at 20℃; for 2h; chemoselective reaction;100%
61-54-1

tryptamine

20698-04-8

3,6-diiodopyridazine

500733-95-9

[2-(1H-indol-3-yl)-ethyl]-(6-iodo-pyridazin-3-yl)-amine

Conditions
ConditionsYield
In iso-butanol for 96h; Heating;100%
61-54-1

tryptamine

2946-89-6

3,5-dimethyl-N-nitro-1H-pyrazole-1-carboxamidine

N-nitro-N'-[2-(1H-indol-3-yl)ethy]guanidine

Conditions
ConditionsYield
In methanol at 20℃;100%
61-54-1

tryptamine

1694-92-4

2-Nitrobenzenesulfonyl chloride

311781-49-4

N-(2-(1H-indol-3-yl)ethyl)-2-nitrobenzenesulfonamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 1.5h;100%
With triethylamine In dichloromethane at 0 - 20℃; for 1h;97%
With N-ethyl-N,N-diisopropylamine In dichloromethane for 0.5h; Inert atmosphere;97%
61-54-1

tryptamine

785-56-8

3,5-bis(trifluoromethyl)phenyl carboxylic acid chloride

372109-22-3

N-(2-(1H-indol-3-yl)ethyl)-3,5-bis(trifluoromethyl)benzamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; Inert atmosphere;100%
With triethylamine In dichloromethane at 22℃; for 16h;
61-54-1

tryptamine

101385-93-7

3-oxo-pyrrolidine-1-carboxylic acid tert-butyl ester

spiro

Conditions
ConditionsYield
Stage #1: tryptamine; 3-oxo-pyrrolidine-1-carboxylic acid tert-butyl ester With acetic acid at 100℃; for 4.5h;
Stage #2: With hydrogenchloride In 1,4-dioxane at 20℃;
100%
61-54-1

tryptamine

66684-58-0

3,4,5-trifluoronitrobenzene

1132682-52-0

C16H13F2N3O2

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine at 120℃; for 18h;100%
61-54-1

tryptamine

24964-64-5

3-Cyanobenzaldehyde

1171311-06-0

3-(2,3,4,9-tetrahydro-1H-pyrido[3,4-b] indol-1-yl)benzonitrile

Conditions
ConditionsYield
With trifluoroacetic acid In 1,1-dichloroethane Reflux;100%
With trifluoroacetic acid In dichloromethane at 20℃; for 24h; Pictet-Spengler Synthesis;18%
61-54-1

tryptamine

6334-18-5

2,3-dichlorobenzylaldehyde

331852-79-0

C17H14Cl2N2

Conditions
ConditionsYield
With trifluoroacetic acid In 1,1-dichloroethane Reflux;100%
61-54-1

tryptamine

13139-14-5

Boc-Trp-OH

1244546-21-1

(S)-Nα-tert-butoxycarbonyl-N-[2-(3-indolyl)ethyl]tryptophanamide

Conditions
ConditionsYield
Stage #1: Boc-Trp-OH With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane for 0.5h; Inert atmosphere;
Stage #2: tryptamine In dichloromethane at 20℃; Inert atmosphere;
100%
61-54-1

tryptamine

C11H22O2Si

1448446-83-0

C21H34N2OSi

Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride In dichloromethane at 0℃; for 12h;100%
61-54-1

tryptamine

96-17-3, 57456-98-1

2-Methylbutyraldehyde

1038257-36-1

N-(2-(1H-indol-3-yl)ethyl)-2-methylbutan-1-amine

Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride In 2-methyltetrahydrofuran at 18℃; for 2h; Solvent; Green chemistry;100%
61-54-1

tryptamine

C73H8F3NO4

C79H15F3N2O

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 20℃; for 5h; Inert atmosphere;100%
61-54-1

tryptamine

35302-72-8

pyrrol-2-yl trichloromethyl ketone

15776-55-3

N-(2-(1H-indol-3-yl)ethyl)-1H-pyrrole-2-carboxamide

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 50℃; for 3h; Inert atmosphere;100%
61-54-1

tryptamine

677-25-8

ethylenesulfonyl fluoride

2,2′-((2-(1H-indol-3-yl)ethyl)azanediyl)diethanesulfonyl fluoride

Conditions
ConditionsYield
In dichloromethane at 20℃;100%
In dichloromethane at 20℃; for 6h;95%
61-54-1

tryptamine

448-61-3

2,4,6-triphenylpyrylium tetrafluoroborate

1-(2-(1H-Indol-3-yl)ethyl)-2,4,6-triphenylpyridin-1-ium tetrafluoroborate

Conditions
ConditionsYield
In ethanol at 85℃;100%
In ethanol at 85 - 90℃; for 4h; Schlenk technique;91%
With acetic acid In dichloromethane at 20℃; Inert atmosphere; Schlenk technique;59%
In ethanol Reflux;
In ethanol at 80 - 85℃; for 4h; Inert atmosphere;
61-54-1

tryptamine

530-78-9

flufenamic acid

C14H10F3NO2*C10H12N2

Conditions
ConditionsYield
In methanol at 20℃;100%
61-54-1

tryptamine

C17H15F3N2O3

C17H15F3N2O3*C10H12N2

Conditions
ConditionsYield
In methanol at 20℃;100%
61-54-1

tryptamine

98-88-4

benzoyl chloride

4753-09-7

N-benzoyltryptamine

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 3h;99%
With sodium hydroxide In acetone at -30℃;95%
In dichloromethane82%
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Specification

The Tryptamine, with the CAS registry number 61-54-1, is also known as 2-Indol-3-yl-aethylamin. It belongs to the product categories of Drug Intermediates; Indole; Indoles; Tryptamines; Amines; Heterocycles; Non-Chiral Heterocyclic Compounds. Its EINECS registry number is 200-510-5. This chemical's molecular formula is C10H12N2 and molecular weight is 160.22. What's more, both its IUPAC name and systematic name are the same which is called 2-(1H-Indol-3-yl)ethanamine. It should be stored in a dry and sealed place at 4 °C. Tryptamine is a monoamine alkaloid found in plants, fungi, and animals. It is found in trace amounts in the brains of mammals and is believed to play a role as a neuromodulator or neurotransmitter.

Physical properties about Tryptamine are: (1)ACD/LogP: 1.542; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): -1.53; (4)ACD/LogD (pH 7.4): -0.81; (5)ACD/BCF (pH 5.5): 1.00; (6)ACD/BCF (pH 7.4): 1.00; (7)ACD/KOC (pH 5.5): 1.00; (8)ACD/KOC (pH 7.4): 1.00; (9)#H bond acceptors: 2; (10)#H bond donors: 3; (11)#Freely Rotating Bonds: 3; (12)Polar Surface Area: 41.81 Å2; (13)Index of Refraction: 1.669; (14)Molar Refractivity: 51.613 cm3; (15)Molar Volume: 138.366 cm3; (16)Polarizability: 20.461×10-24cm3; (17)Surface Tension: 54.728 dyne/cm; (18)Density: 1.158 g/cm3; (19)Flash Point: 187.672 °C; (20)Enthalpy of Vaporization: 62.67 kJ/mol; (21)Boiling Point: 378.766 °C at 760 mmHg; (22)Vapour Pressure: 0 mmHg at 25 °C.

Uses of Tryptamine: it is used to produce other chemicals. For example, it can react with 1H-benzo[d][1,3]oxazine-2,4-dione to get 2-amino-N-(2-indol-3-yl-ethyl)-benzamide. This reaction needs solvent acetonitrile at ambient temperature. The reaction time is 3 hours. The yield is 92.7 %.

Tryptamine can react with 1H-benzo[d][1,3]oxazine-2,4-dione to get 2-amino-N-(2-indol-3-yl-ethyl)-benzamide.

When you are dealing with this chemical, you should be very careful. This chemical may cause inflammation to the skin or other mucous membranes. It is harmful by inhalation, in contact with skin and if swallowed. In addition, it is irritating to eyes, respiratory system and skin. Therefore, you should wear suitable protective clothing, gloves and eye/face protection. You must avoid contacting with skin and eyes. In case of contacting with eyes, you should rinse immediately with plenty of water and seek medical advice.

You can still convert the following datas into molecular structure:
(1) SMILES: c1ccc2c(c1)c(c[nH]2)CCN
(2) InChI: InChI=1S/C10H12N2/c11-6-5-8-7-12-10-4-2-1-3-9(8)10/h1-4,7,12H,5-6,11H2
(3) InChIKey: APJYDQYYACXCRM-UHFFFAOYSA-N

The toxicity data is as follows:

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mouse LD50 intraperitoneal 100mg/kg (100mg/kg)   European Journal of Medicinal Chemistry--Chimie Therapeutique. Vol. 9, Pg. 453, 1974.
mouse LD50 subcutaneous 500mg/kg (500mg/kg) BEHAVIORAL: SOMNOLENCE (GENERAL DEPRESSED ACTIVITY) Dissertationes Pharmaceuticae et Pharmacologicae. Vol. 22, Pg. 313, 1970.
rat LD50 intraperitoneal 223mg/kg (223mg/kg)   Journal of Pharmaceutical Sciences. Vol. 66, Pg. 1692, 1977.