Organometallics p. 3588 - 3591 (1995)
Update date:2022-09-26
Topics:
Nikonov, Georgii I.
Kuzmina, Ludmila G.
Mountford, Philip
Lemenovskii, Dmitry A.
Ph2PCl easily inserts into the Ta-H bond of Cp2TaH3 affording an ionic complex [Cp2TaH2(HPPh2)]Cl (4). This species was deprotonated to give the first phosphido-substituted tantalocene complex Cp2TaH2PPh2 (5), which was characterized by NMR spectroscopy and X-ray crystallography. Thermal decomposition of 5 as well as its reaction with HPPh2 was studied.
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