Journal of Organic Chemistry p. 4132 - 4141 (2015)
Update date:2022-08-05
Topics:
Gatineau, David
Nguyen, Duc Hanh
Hérault, Damien
Vanthuyne, Nicolas
Leclaire, Julien
Giordano, Laurent
Buono, Gérard
A new family of H-adamantylphosphinates as universal precursors of P-stereogenic ligands was obtained in one step from commercial chlorophosphines. Both enantiomers of these air- and moisture-stable intermediates can easily be separated by semipreparative chiral HPLC on a gram scale and individually undergo stereoselective transformations to afford each enantiomer of a set of P-stereogenic compounds such as secondary phosphine oxides and boron-protected monophosphines.
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