Journal of the American Chemical Society p. 1908 - 1939 (1995)
Update date:2022-09-26
Topics:
White, James D.
Bolton, Gary L.
Dantanarayana, Anura P.
Fox, Christina M. J.
Hiner, Roger N.
Jackson, Randy W.
Sakuma, Kazuhiko
Warrier, Ulhas S.
The synthesis of avermectin B1a has been completed by a route that assembles the aglycon from three subunits consisting of the hexahydrobenzofuran moiety (A), the spiroketal segment (B), and the acyclic portion (C) comprising C9-C15. Connection is made in a B + C → (B -C) + A sequence, and the synthesis is concluded by attachment to the aglycon of the L-oleandrosyl-L-oleandrose disaccharide via the pyridylthio glycoside.
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