Bulletin of the Chemical Society of Japan p. 2331 - 2348 (1995)
Update date:2022-07-30
Topics:
Koto, Shinkiti
Haigoh, Hisamitsu
Shichi, Sonoko
Hirooka, Motoko
Nakamura, Teiko
et al.
Glycogen-storage-disease-relating linear tetra-, hexa-, and octasaccharides of D-glucose having α(1->4) and α(1->6) linkages were synthesized using a stereoselective dehydrative glycosylation with a reagent mixture of p-nitrobenzenesulfonyl chloride, silver trifluoromethanesulfonate, N,N-dimethylacetamide, and triethylamine.A cross-condensation of a quasi-stoichiometric amount of a donor and an acceptor of an octasaccheride, followed by deprotection, afforded a glucohexadecasaccharide.
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(1995)
