Journal of Organometallic Chemistry p. 2029 - 2032 (2004)
Update date:2022-08-03
Topics:
Ariyaratne, Kanahara A.N.S.
Cramer, Roger E.
Jameson, Geoffrey B.
Gilje, John W.
The reaction of Cp*2UCl2(HNSPh2) with HNSPh2·H2O in 1:1 stoichiometry, produces Cp*2UCl(OH)(HNSPh2) in good yield. This is the first structurally characterized metallocene f-element complex containing a terminal hydroxy ligand. Cp*2UCl(OH)(HNSPh2) is an intermediate in the formation of a tetra uranium-oxo-cluster [Cp*(Cl)(HNSPh2)U(μ3-O) (μ2-O)2U(Cl)(HNSPh2) 2]2, which forms by hydrolysis of Cp*2UCl2 with excess HNSPh2·H2O.
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