Tetrahedron Letters p. 707 - 710 (1996)
Update date:2022-07-29
Topics:
Eames, Jason
Jones, Ray V. H.
Warren, Stuart
New routes to cyclic and spirocyclic sulfides involve aldol reactions of dithioesters or chemoselective Mitsunobu reactions on diols to give 2-hydroxyalkyl sulfides with a terminal SH group. Treatment with acid gives cyclic sulfides, or by rearrangement with S migration, spirocyclic sulfides or allylic sulfides in good yield.
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(1996)
