Journal of Carbohydrate Chemistry p. 857 - 878 (1996)
Update date:2022-08-03
Topics:
Kondo, Tadao
Tomoo, Toshiyuki
Abe, Hiroyuki
Isobe, Minoru
Goto, Toshio
Glycosylation of an 8-unprotected sialyl fluoride 16 with 2β-chloro-3β-phenylthio-Neu5Ac 2 gave the desired α-disialate 23. Subsequent glycosylation of a thiolactoside 19 with the disialyl fluoride 23 gave the tetrasaccharide 28. Synthesis of GD3 1 was realized by condensation of the tetrasaccharide 28 with azidosphingosine 31, following our previously reported GM3 synthesis procedure.
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