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Lipase-Catalyzed Resolution of 2-Substituted 3-Cyclopenten-1-ol Derivatives

DOI: 10.1246/cl.1991.1651

Source and publish data:

Chemistry Letters p. 1651 - 1652 (1991)

Update date:2022-08-04

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Authors:

Sakai, TakashiSakai, Takashi

Iida, YasuhiroIida, Yasuhiro

Kikuyama, ShigekiKikuyama, Shigeki

Tsuboi, SadaoTsuboi, Sadao

Utaka, MasanoriUtaka, Masanori

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Article abstract of DOI:10.1246/cl.1991.1651

2-Oxabicyclo<3.3.0>oct-6-en-3-one, the key intermediate in the prostaglandin synthesis, was subjected to the optical resolution effectively by use of lipase after conversion to 2-<2-(t-butyldimethylsilyloxy)ethyl>-3-cyclopenten-1-yl acetate and 2-<2-(N,N-dimethylcarbamoyl)methyl>-3-cyclopenten-1-yl-acetate.

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Full text of DOI:10.1246/cl.1991.1651

Products guided by the article

Product name:(1S,2R)-2-[2-(tert-Butyl-dimethyl-silanyloxy)-ethyl]-cyclopent-3-enol

Cas No:180187-46-6

180187-46-6

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