Preparation of 3-amino-1,4-benzodiazepin-2-ones via direct azidation with trisyl azide

DOI: 10.1016/S0040-4039(96)01475-X

Source and publish data:

Tetrahedron Letters p. 6685 - 6688 (1996)

Update date:2022-07-29

Topics:

Authors:

Butcher, John W.

Liverton, Nigel J.

Selnick, Harold G.

Elliot, Jason M.

Smith, Garry R.

Tebben, Andrew J.

Pribush, David A.

Wai, John S.

Claremon, David A.

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Article abstract of DOI:10.1016/S0040-4039(96)01475-X

An efficient synthesis of 3-amino-1,4-benzodiazepin-2-ones utilizing triisopropylbenzenesulfonyl azide (trisyl azide) for the direct azidation of 1,4-benzodiazepin-2-ones is described.

Full text of DOI:10.1016/S0040-4039(96)01475-X

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Product name:3-amino-1-phenyl-5-(2-propyl)-1,5-benzodiazepin-2,4-dione

Cas No:182436-37-9

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