Chemical and Pharmaceutical Bulletin p. 2153 - 2156 (1996)
Update date:2022-08-03
Topics: Molecular structure Column chromatography Reagents Catalyst Stereoselective synthesis Chemical reactions Purification Chirality Side chain
Chen, Cheng Yu
Nagumo, Shinji
Akita, Hiroyuki
Optically pore (3R,7R)-3,7,11-trimethyldodecan-1-ol (16), corresponding to the α-tocopherol side chain, was synthesized by the coupling reaction of a chiral isoprene unit (3S)-9 derived from an enzymatically hydrolyzed product (2S,3S)-2 and a ten-carbon alkylating reagent (R)-13 derived from (R)-(+)-pulegone.
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Doi:10.1039/c2cc17836b
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(1991)
