Synthesis of ubiquinones-3 specifically labelled with 13C at C(5)- or C(6)-positions

DOI: 10.1016/S0040-4020(96)01181-7

Source and publish data:

Tetrahedron p. 2505 - 2512 (1997)

Update date:2022-08-03

Topics:

Authors:

Boullais, Claude

Breton, Jacques

Nabedryk, Eliane

Mioskowski, Charles

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Article abstract of DOI:10.1016/S0040-4020(96)01181-7

(5-¹³C) and (6-¹³C) ubiquinones-3 (20a and 20b) were synthesised from (1-¹³C) trichloroacetic acid (8a) in 12 steps. The key step was a Diels Alder reaction between 2,5-bis (trimethylsilyloxy)-3-methylfuran (2) and (2- View More

Full text of DOI:10.1016/S0040-4020(96)01181-7

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