Tetrahedron p. 9769 - 9776 (1997)
Update date:2022-08-03
Topics:
Kabeya, Mototsugu
Hamada, Yasumasa
Shioiri, Takayuki
A simple and safe route to the D-xylone-l,4-lactone derivative 3, a key intermediate for the synthesis of the spiroketal fragment in calyculin A (I) has been explored without the use of hazardous diazomethane on a large scale.
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Doi:10.1021/jo970575n
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