Synthesis of γ-lactone derivatives as a key intermediate for the spiroketal fragment in calyculin A

DOI: 10.1016/S0040-4020(97)00624-8

Source and publish data:

Tetrahedron p. 9769 - 9776 (1997)

Update date:2022-08-03

Topics:

Authors:

Kabeya, Mototsugu

Hamada, Yasumasa

Shioiri, Takayuki

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Article abstract of DOI:10.1016/S0040-4020(97)00624-8

A simple and safe route to the D-xylone-l,4-lactone derivative 3, a key intermediate for the synthesis of the spiroketal fragment in calyculin A (I) has been explored without the use of hazardous diazomethane on a large scale.

Full text of DOI:10.1016/S0040-4020(97)00624-8

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