Tetrahedron Letters p. 749 - 752 (1998)
Update date:2022-09-26
Topics:
Johns, Brian A.
Johnson, Carl R.
Double Suzuki coupling was achieved with vinyl bromide 7, synthesized from the bromobenzene microbial oxidation metabolite bromocyclohexadienediol 6 and α,ω-diborane coupling partners derived from the hydroboration of the corresponding diene. Ozonolysis and selective reduction protocols served to provide selectively the α/α or β/β tethered polyhydroxylated piperidine ring systems (bis-azabugars). The C8 linked DMJ analogue 1 showed inhibitory activity against glycosidase enzymes.
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(1998)
