Tetrahedron p. 2059 - 2074 (1998)
Update date:2022-08-05
Topics:
Hiebl, Johann
Blanka, Michael
Guttman, Andras
Kollmann, Hermann
Leitner, Kornelia
Mayrhofer, Guenter
Rovenszky, Franz
Winkler, Karin
The yield of protected 2,7-diaminosuberic acid (DAS) prepared by Kolbe reaction of N-protected α-glutamic acid esters is dependent on solvent, temperature, concentration of carboxylate onion, and protecting groups. The highest yield of protected L,L-2,7-diaminosuberic acid is obtained with Boc-Glu-OMe as starting material using MeOH/pyridine/NaOMe as electrolyte.
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Doi:10.1039/a707881a
(1998)Doi:10.1271/bbb1961.44.2913
(1980)Doi:10.1016/S0040-4039(98)00041-0
(1998)Doi:10.1016/S0968-0896(00)00046-8
(2000)Doi:10.1016/S0040-4020(98)00067-2
(1998)Doi:10.1039/a706354g
(1998)
