Synlett p. 869 - 872 (1998)
Update date:2022-09-26
Topics:
Kocienski, Philip J.
Narquizian, Robert
Raubo, Piotr
Smith, Christopher
Boyle, F. Thomas
Mycalamide B, a potent antitumour agent, was synthesised from cheap, readily available starting materials: ethyl lactate, ethyl isobutyrate, 4-chlorobutanal, and 4-chlorobutanoyl chloride. The trioxabicyclo[4.4.0]decane ring system was created by reaction of a methoxymethyl ether with a silyloxyoxirane induced by phosphorus pentoxide.
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(2017)Doi:10.1021/acs.jmedchem.6b01433
(2016)Doi:10.1039/b803314e
(2008)Doi:10.1016/j.bmcl.2009.12.097
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(2014)Doi:10.1016/j.tet.2008.03.032
(2008)