Synthesis of aminophenyl and methoxyphenyl perfluoroalkyl ketones

DOI: 10.1016/S0022-1139(98)00230-9

Source and publish data:

Journal of Fluorine Chemistry p. 221 - 224 (1998)

Update date:2022-08-04

Topics:

Authors:

Lee, Hyeran

Czarny, Agnieszka

Battiste, Merle A.

Strekowski, Lucjan

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Article abstract of DOI:10.1016/S0022-1139(98)00230-9

The title compounds are obtained by direct hydrolysis of the corresponding 2/4-perfluoroalkyl-substituted anilines and anisoles by the system AcOH/HBr/H₂O/Al₂O₃. A two-step preparation of 2/4-perfluoroacylanilines involves the treatment of the 2/4-perfluoroalkylaniline with sodium ethoxide followed by hydrolysis of the resultant diethyl acetal with hydriodic acid.

Full text of DOI:10.1016/S0022-1139(98)00230-9

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