Tetrahedron p. 989 - 1004 (1999)
Update date:2022-08-03
Topics:
Murakami, Teiichi
Taguchi, Kazuhiro
D-ribo-Phytosphingosine 1 was conveniently synthesized from N-benzoyl- D-glucosamine 3 by an improved route in which regioselective O- methanesulfonation and diastereoselective Grignard addition are involved as key steps. Using a synthetic intermediate of 1, novel D-ribo- phytosphingosine-type glycolipids 2a and 2b, unnatural homologues of antifungal cerebrosides Halicylindrosides, were efficiently synthesized in a stereocontrolled manner.
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Doi:10.1016/S0040-4039(98)80050-6
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(2021)Doi:10.1002/anie.202107182
(2021)
