Tetrahedron p. 1921 - 1936 (1999)
Update date:2022-08-05
Topics:
Riedel, Sylvia
Donnerstag, Astrid
Hennig, Lothar
Welzel, Peter
Richter, Joachim
Hobert, Kurt
Mueller, Dietrich
Van Heijenoort, Jean
A disaccharide analogue (A4 = 13c) of moenomycin A lacking the OH group in the 4-position of the uronic acid moiety has been synthesized using the Saito deoxygenation reaction as key step. 13c does not inhibit the transglycosylase (PBP 1b), a key enzyme in the biosynthesis of bacterial peptidoglycan. The result demonstrates the importance of this OH group for the binding of disaccharide moenomycin analogues to the enzyme.
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(2008)
