Fluorination of Nitro Compounds with Acetyl Hypofluorite

DOI: 10.1021/jo00101a047

Source and publish data:

Journal of Organic Chemistry p. 6800 - 6803 (1994)

Update date:2022-07-30

Topics:

Authors:

Rozen, Shlomo

Bar-Haim, Arie

Mishani, Eyal

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Article abstract of DOI:10.1021/jo00101a047

Various types of nitro derivatives are fluorinated to form the CFNO2 moiety in very good yields using acetyl hypofluorite (AcOF).The corresponding nitro anion, preferably prepared with NaOMe, is added quickly to a cold (-75 deg C) CFCl3 solution of AcOF,

Full text of DOI:10.1021/jo00101a047

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