Russian Chemical Bulletin p. 1295 - 1298 (1999)
Update date:2022-08-05
Topics:
Frumkin
Churakov
Strelenko
Smirnov
Ioffe
Tartakovsky
Oxidation of 4,6-dichloro-1,3-phenylenediamine with Caro's acid yields the corresponding dinitrosobenzene, which reacts with N,N-dibromo-tert-butylamine to give 1,5-bis(tert-butyl-NNO-azoxy)-2,4-dichlorobenzene. Treatment of the latter with ammonia yields 4-amino-and 4,6-diamino-1,3-bis(tert-butyl-NNO-azoxy)benzenes.
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(1999)Doi:10.1016/S0957-4166(99)00321-3
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(1999)
