Synlett p. 2018 - 2023 (2017)
Update date:2022-08-03
Topics:
Shao, Tongle
Fang, Xiang
Zhou, Jun
Jin, Chen
Yang, Xueyan
Wu, Fanhong
A metal-free oxidative coupling reaction of trifluoromethyl β-diketones with alcohols for the synthesis of α-keto esters in good to excellent yields has been developed. Preliminary mechanistic studies suggest that an I 2 /TBHP promoted sequential iodination, C-C bond cleavage, C-O bond formation and oxidation pathway is involved in this reaction.
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