Organic Process Research and Development p. 28 - 32 (2004)
Update date:2022-09-26
Topics: Green chemistry Scalability Catalyst Immobilization Precise Control of Reaction Conditions Enhanced Safety Continuous Flow Chemistry
Wiles, Charlotte
Watts, Paul
Haswell, Stephen J.
Pombo-Villar, Esteban
We demonstrate the successful synthesis of an array of 1,2-azoles within a borosilicate glass microreactor whereby conversions in the range of 98-100% were obtained. In terms of large-scale production, this corresponds to 0.339 g day-1 per microreactor when employing reagent concentrations of 1.0 M.
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