Tetrahedron Letters p. 6513 - 6516 (1999)
Update date:2022-08-04
Topics:
Trauner, Dirk
Danishefsky, Samuel J.
The C1-C15 spiroquinolizidine subunit (cf. 2) of the marine natural product halichlorine (1) was prepared in 12 steps starting from the known 'Meyers-lactam' 5. The synthesis involves a B-alkyl-Suzuki coupling followed by a highly stereoselective intramolecular Michael addition and an intramolecular Mannich ring closure.
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