Journal of Organic Chemistry p. 1340 - 1346 (2017)
Update date:2022-08-05
Topics:
You, Tingjie
Wang, Zhenrong
Chen, Jiajia
Xia, Yuanzhi
A simple and efficient Ru(II)-catalyzed transfer hydro-dehalogenation of organic halides using 2-propanol solvent as the hydride source was reported. This methodology is applicable for hydro-dehalogenation of a variety of aromatic halides and α-haloesters and amides without additional ligand, and quantitative yields were achieved in many cases. The potential synthetic application of this method was demonstrated by efficient gram-scale transformation with catalyst loading as low as 0.5 mol %.
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Doi:10.1016/S0040-4039(00)80832-1
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