Chemical Communications p. 16561 - 16564 (2015)
Update date:2022-08-04
Topics:
Kenny, Niall P.
Rajendran, Kamalraj V.
Gilheany, Declan G.
A method is reported for the phosphoryl bond cleavage of O-alkyl phosphinates, phosphinothioates and certain phosphonamidates to furnish the corresponding P(iii) borane adducts. The two-step procedure relies upon initial activation of the phosphoryl bond with an alkyl triflate, followed by reduction of the resulting intermediate using lithium borohydride.
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