Preparation and Crystal Structure of 3> and an Improved Route to

DOI: 10.1039/DT9830000397

Source and publish data:

Journal of the Chemical Society, Dalton Transactions p. 397 - 398 (1983)

Update date:2022-07-30

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Authors:

Dilworth, Jonathan R.

Zubieta, Jon A.

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Article abstract of DOI:10.1039/DT9830000397

The complex (thf = tetrahydrofuran) is prepared in high yield by the tin reduction of in thf.It reacts with in dry methanol to give 3> which crystallizes in the space group C2/c with a = 14.342(5), b = 11.239(5), c = 12.945(4) Angstroem, β = 97.12(1) deg, and Z = 4. 2 453 Reflections gave R = 0.039.The molybdenum is pseudo-octahedral and the complex has overall C2 symmetry.The Mo-S average distance is 2.507(2) Angstroem.

Full text of DOI:10.1039/DT9830000397

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