Tetrahedron Letters p. 7231 - 7234 (1993)
Update date:2022-08-05
Topics:
Curphey, Thomas J.
Joyner, H. Howard
Reaction of 3-oxo dithioic acids with a combination of hexamethyldisilathiane and N-chlorosuccinimide in the presence of a catalytic amount of imidazole brings about oxidative ring closure to 3H-1,2-dithiole-3-thiones. Yields vary from poor to good.
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