Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry p. 665 - 687 (2002)
Update date:2022-08-05
Topics:
Ahmad, Fiaz
Parvez, Masood
Ali, Saqib
Mazhar
Munir, Arshad
A series of tri- and diorganotin(IV) complexes of the general formula R4-nSnLn (where R = CH3, C4H9, C6H6, C7H7, n = 1, 2 and HL = 5-benzoyl-α-methyl-2-thiopheneacetic acid) have been sythesized by the reaction of tri- and diorganotin(IV) chloride(s) with the silver salt of the ligand in CHCl3 solution. All of the compounds have been characterized by IR, conductance measurement, multinuclear (1H, 13C, 119Sn) NMR, UV-Vis and mass spectrometery. An X-ray crystal structure of the representative compound (CH3)3SnL confirms a trigonal bipyramid around the tin atom, having the space group P21/a with a monoclinic crystal system.
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Doi:10.1016/S0040-4039(00)95565-5
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