Phosphorus, Sulfur and Silicon and the Related Elements p. 220 - 224 (2011)
Update date:2022-07-30
Topics: Solvent-free one-pot synthesis Eco-Friendly Catalyst-Free Experimental terms 2,4-disubstituted thiazoles Grinding
Ding, Quansehng
Zhu, Dongjian
Jin, Huile
Chen, Jiuxi
Ding, Jinchang
Wu, Huayue
Chemical Equation Presented An efficient and facile synthesis of 2,4-disubstituted thiazoles is achieved by a one-pot reaction of aldehydes and α-bromoketones with thiosemicarbazide by grinding under catalyst- and solvent-free conditions. This method has notable advantages in terms of simple workup, neat conditions, high yield, reasonably rapid reaction rate, and environmental friendliness. Supplemental materials are available for this article. Go to the publisher's online edition of Phosphorus, Sulfur, and Silicon and the Related Elements to view the free supplemental file. Copyright Taylor & Francis Group, LLC.
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