Journal of labelled compounds p. 339 - 346 (1973)
Update date:2022-08-04
Topics:
Bell
Scott
The synthesis of 25 hydroxycholecalciferol (26,27 3H) is described. 25 oxo 27 norcholesta 5,7 dien 3β yl acetate is converted photochemically to 25 oxo 27 norcholecalciferol 3 acetate, which is then reacted with tritiated methylmagnesium iodide and subsequently saponified to give 25 hydroxycholecalciferol (26,27 3H).
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Doi:10.1021/jo01340a039
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(2018)Doi:10.1002/ejoc.202000871
(2020)Doi:10.1016/S0968-0896(03)00083-X
(2003)Doi:10.1021/jo00925a001
(1974)
