Bulletin of the Academy of Sciences of the USSR Division of Chemical Science p. 2377 - 2382 (1989)
Update date:2022-09-26
Topics:
Ragulin, V. V.
Bofanova, M. E.
Tsvetkov, E. N.
A method is described for the synthesis of phosphorus-containing amino carboxylic acids, by the Michaelis-Bekker or Arbuzov phosphorylation of ω-haloalkylacetamidomalonic ester.The latter were obtained by alkylating the sodium salt of acetamidomalonic ester with an excess of the α,ω-dihaloalkane.Acid hydrolysis of the phosphorus-containing alkylacetamidomalonic esters gave the required compounds.
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