Tetrahedron Letters p. 1627 - 1629 (2003)
Update date:2022-08-03
Topics:
Bashford, Katherine E.
Burton, Matthew B.
Cameron, Stuart
Cooper, Anthony L.
Hogg, Rebecca D.
Kane, Peter D.
MacManus, David A.
Matrunola, Christopher A.
Moody, Christopher J.
Robertson, Avril A. B.
Warne, Mark R.
The Bohlmann-Rahtz reaction has been used to prepare 2,3,6-trisubstituted pyridines suitable for use in library synthesis. The synthesis of piperidine substituted nicotinic acid derivative 9 has been optimised and carried out on a large scale to give ca. 500 g of scaffold which was used in the generation of the pyridine library 11.
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