Acta Crystallographica, Section C: Crystal Structure Communications p. 2710 - 2713 (1996)
Update date:2022-09-26
Topics:
Ferguson, George
Mceneaney, Patricia A.
Spalding, Trevor R.
Ontario
The title compound, [3,3-(PPh3)2-3-Cl-3,1,1,2-RhC2B 9H11] or [RhCl(C2H11B9)(C18H 15P)2]. 1.1CH2Cl2, contains a triangulated icosahedral closo-RhC2B9 cage. Principal bond distances are Rh - Cl 2.423 (2), Rh - P 2.373 (2) and 2.383 (2), Rh - C 2.190 (6) and 2.191 (6), and Rh - B 2.203 (8)-2.289 (8) A. The conformation of the Rh(PPh3)2Cl group above the C2B3 face of the dicarbaborane ligand is such that the Rh - Cl bond is located above the cage C - C vector.
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