A new way to prepare Grignard reagent from RX (X = Cl,Br) using the mixture of BrCH2CH2Br and I2 as an initiator

Article abstract of DOI:10.1080/00397919908086069

Grignard reagents (RMgX) were prepared from RX (X = Cl,Br) using the mixture of BrCH₂CH₂Br and I₂ as an initiator in anhydrous solvent such as THF or ether. The rate of preparing Grignard reagent was increased because of using the mixture of BrCH₂CH₂Br and I₂ as an initiator.

Full text of DOI:10.1080/00397919908086069

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Synthetic Communications: An
International Journal for Rapid
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Organic Chemistry
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A New Way to Prepare
Grignard Reagent from RX
(X=Cl,Br) Using the Mixture
of BrCH2CH2Br and I2 as an
Initiator
Li Jing a , Liao Xiangjun a , Liu Hua a , Xie Qinglan a ,
Liu Zhun a & He Xilin b
a Research Institute of Elemento-Organic Chemistry,
Nankai University , Tianjin, 300071, P.R.China
b Department of Chemistry Nus , Singapore , 119260
Published online: 17 Sep 2007.
To cite this article: Li Jing , Liao Xiangjun , Liu Hua , Xie Qinglan , Liu Zhun &
He Xilin (1999) A New Way to Prepare Grignard Reagent from RX (X=Cl,Br) Using
the Mixture of BrCH2CH2Br and I2 as an Initiator, Synthetic Communications: An
International Journal for Rapid Communication of Synthetic Organic Chemistry, 29:6,
1037-1039, DOI: 10.1080/00397919908086069
To link to this article: http://dx.doi.org/10.1080/00397919908086069
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