CHLORINE-35 NUCLEAR QUADRUPOLE RESONANCE STUDIES ON SOME TIN(IV) CHLORIDE ADDUCTS

DOI: 10.1039/DT9800001164

Source and publish data:

Journal of the Chemical Society, Dalton Transactions p. 1164 - 1168 (1980)

Update date:2022-08-04

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Authors:

Huggett, Paul G.

Lynch, Roderick J.

Waddington, Thomas C.

Wade, Kenneth

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Article abstract of DOI:10.1039/DT9800001164

The ³⁵Cl n.q.r. spectra of a series of tin(IV) chloride adducts SnCl4*2L tCN, PhCN'CH2(CN)2, 1,2-C6H4(CN)2, SMe2O, or tht (tetrahydrothiophen)> have been recorded at variuos temperatures and used to deduce whether these complexes are cis or trans.A trans structure is indicated for SnCl4*2tht, cis structures for the remainder.When compared with other published n.q.r. and structural data, our results indicate that the ³⁵Cl n.q.r. frequencies are related to the Sn-Cl bond lengths in such systems.The higher ³⁵Cl n.q.r. frequencies tend to be associated with the shorter bonds, though the frequencies also vary markedly with temperature.

Full text of DOI:10.1039/DT9800001164

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